Reacción #1344314

ord-e714056c8ea14213a8ec2ddd553539a4

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    TemperaturaThe microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W
  2. 2
    Otrohydrolysis reaction for no more than 20 minutes

Procedimiento

The 2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene and NaOH are mixed in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W to perform hydrolysis reaction for no more than 20 minutes to obtain 2,5-dicarboxy-3,4-ethylenedioxythiophene. The reaction is shown in the chemical formula (D).

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08461355B2uspto-grants-2013_06