Reacción #1340988

ord-ba72d94d7963431fb2906229b41a3326

Ecuación de reacción

Cc1c(Br)cnc(O)c1C
5-bromo-3,4-dimethylpyridin-2-ol
Cc1ccc(S(=O)(=O)OCCC(C)(C)O)cc1
3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate
Cc1c(Br)cnc(OCCC(C)(C)O)c1C
compound
Rendimiento 49.1%
Cc1c(Br)cnc(OCCC(C)(C)O)c1C
4-(5-bromo-3,4-dimethylpyridin-2-yl)oxy-2-methylbutan-2-ol
Rendimiento 49.1%

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

According to the method of (Example 36) <Step 1>, from 5-bromo-3,4-dimethylpyridin-2-ol (3.0 g) and 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate (4.2 g), the subject compound (2.1 g) was obtained as a white solid.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08455500B2uspto-grants-2013_06