Reacción #1340577

Ecuación de reacción

octadecyl succinic anhydride

ethanolamine

→

N-(2-hydroxyethyl)octadecyl succinimide

Rendimiento 54.0%

Condiciones de reacción

Tratamiento posterior

1. 1
   OtroA 50 mL reaction flask
2. 2
   Otrothe resulting mixture was reacted at 160° C. for 4 hours under continuous nitrogen purging and with vigorous stirring
3. 3
   OtroThe reaction product was purified by silica gel column chromatography (mobile phase: ethyl acetate/hexane)

Procedimiento

A 50 mL reaction flask was charged with 17.6 g of octadecyl succinic anhydride (manufactured by Tokyo Chemical Industry Co., Ltd.) and 3.1 g of ethanolamine (manufactured by Tokyo Chemical Industry Co., Ltd.), and the resulting mixture was reacted at 160° C. for 4 hours under continuous nitrogen purging and with vigorous stirring. The reaction product was purified by silica gel column chromatography (mobile phase: ethyl acetate/hexane), yielding 10.6 g of N-(2-hydroxyethyl)octadecyl succinimide (yield: 54%).

Fuente