Reacción #1332452

Ecuación de reacción

2,5-difluoro(4-(trans-4-propylcyclohexyl)cyclohexenyl)benzene

→

titled compound

2,5-difluoro-(4-(trans-4-propylcyclohexyl)cyclohexyl)benzene

Disolventes

ethyl acetate

Condiciones de reacción

Tratamiento posterior

1. 1
   Otrothe absorption of hydrogen, 5% palladium carbon
2. 2
   Filtraciónis filtered off from the reaction mixture
3. 3
   ConcentraciónThe filtrate is concentrated under reduced pressure
4. 4
   Otropurified by silica-gel chromatography
5. 5
   Otrofurther recrystallized

Procedimiento

A mixture of 2,5-difluoro(4-(trans-4-propylcyclohexyl)cyclohexenyl)benzene (0.84 mmol), ethyl acetate (30 ml), and 5% palladium carbon (0.013 g) is stirred under an atmosphere of hydrogen. After ceasing the absorption of hydrogen, 5% palladium carbon is filtered off from the reaction mixture. The filtrate is concentrated under reduced pressure and purified by silica-gel chromatography, and further recrystallized to give the titled compound.

Fuente