Reacción #1277971

ord-50741cdd210a4d198527218adf03e46c

Ecuación de reacción

CCCCOP(=O)(OCCCC)OCCCC
TBPA
CC(N)(CO)CO
AMPD
CC(N)(CO)CO.CCCCOP(=O)(OCCCC)OCCCC
TBPA AMPD

Reactantes

Reactivos

Ninguno

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

Reaction of TBPA with AMPD gives an TBPA/AMPD adduct. AMPD is sold in commerce by Angus. 37.2 mmol of TBPA was combined with 37.2 mmol of AMPD in 164.5 g of pure ethanol. The mixture is refluxed for 2 hours. The solvent was removed using a rotary evaporator to produce a white solid.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08679990B2uspto-grants-2014_03