Reacción #1256745

Ecuación de reacción

Compound 40a

Isobutyldiisopropylsilane

diisopropylchlorosilane

→

Compound 44a

Cyclopropyldiisopropylsilane

Disolventes

Condiciones de reacción

Procedimiento

The procedure of synthesizing Compound 40a was repeated, except that diisopropylchlorosilane (4.10 mL, 96.0 mmol) and cyclopropylmagnesium bromide THF solution (1.0M, 100 mL) were employed, whereby the Compound 44a was obtained as a colorless liquid (boiling point; 35 mmHg, 86 to 89° C. fraction, 1.84 g, 50%).

Fuente