Reacción #1253208

ord-fb11b0cd2b134735807b142cc50ef4bc

Ecuación de reacción

O
water
CC(=O)O
acetic acid
O
water
CN1CCCC1
1-methylpyrrolidine
C1CCNCC1.CC(=O)O
piperidine acetate

Disolventes

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    Concentraciónconcentration

Procedimiento

A stock solution of 1 molar piperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent 1-methylpyrrolidine. The pH of the stock solution is 7. The stock solution was diluted in an appropriate volume of water or acetonitrile to working concentration.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US06613508B1uspto-grants-2003_09