Reacción #1178206

Ecuación de reacción

4-chlorobenzoyl isothiocyanate

2-aminobenzamide

→

N-[[[2-(aminocarbonyl)phenyl]amino]thioxomethyl]-4-chlorobenzamide

Rendimiento 85.8%

Disolventes

tetrahydrofuran

tetrahydrofuran

Condiciones de reacción

Tratamiento posterior

1. 1
   workup.ADDITIONwas added
2. 2
   Otrowas collected

Procedimiento

To a stirred mixture of 10.5 g of 4-chlorobenzoyl isothiocyanate in 100 ml of tetrahydrofuran was added a mixture of 6.8 g of 2-aminobenzamide in 200 ml of tetrahydrofuran. After stirring for 3 hours the solid was collected, giving 14.3 g of N-[[[2-(aminocarbonyl)phenyl]amino]thioxomethyl]-4-chlorobenzamide.

Fuente