Reacción #1135813

Ecuación de reacción

1-ethoxy-2-methyl-3-nitrobenzene

→

3-ethoxy-2-methylaniline

Disolventes

ethanol

Condiciones de reacción

Tratamiento posterior

1. 1
   FiltraciónThe mixtures were filtered
2. 2
   Concentraciónthe filtrates were concentrated

Procedimiento

A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.

Fuente