Reacción #1121771

Ecuación de reacción

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

Condiciones de reacción

Tratamiento posterior

1. 1
   Temperaturawas heated
2. 2
   Temperaturaat reflux for 90 mins
3. 3
   ConcentraciónThe reaction mixture was concentrated under reduced pressure
4. 4
   Otroto give an oil
5. 5
   Otroyield 5.77 parts of the following structure

Procedimiento

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 90 mins. The reaction mixture was concentrated under reduced pressure to give an oil, yield 5.77 parts of the following structure.

Fuente