Reacción #1106669

ord-f5ff3aa120644be0be915121f0436399

Ecuación de reacción

CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
Compound 17
CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
1-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione
COCCN
2-methoxyethylamin
COCCNc1cccc2c1C(=O)c1cccc(NCCN(C)C)c1C2=O
2-(dimethylamino) ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Tratamiento posterior

  1. 1
    OtroThis product was used in the next step without any purification

Procedimiento

This procedure was carried out as described previously in step (a) of Example 15, using Compound 17 (0.25 g, 0.76 mmol) and 2-methoxyethylamin (0.66 mL, 7.6 mmol). This product was used in the next step without any purification. The structure of Compound 23 is given below:

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US08715944B2uspto-grants-2014_05