Reacción #10544
ord-a37b355baf0d4ccb87189a29d7e7e818
Ecuación de reacción
cyclopentylamine
acetone
→
title compound
N-Isopropylcyclopentanamine
Reactantes
Reactivos
Condiciones de reacción
Condiciones detalladas
See reaction.notes.procedure_details.
Tratamiento posterior
- 1workup.STIRRINGAfter stirring for 16 hours the reaction mixture
- 2Filtraciónwas filtered through Arbocel (trade mark)
- 3Otrothe solvent removed under reduced pressure
Procedimiento
Peariman's catalyst (20% w/w palladium hydroxide-on-carbon) (1.5 g) was added to a solution of cyclopentylamine (15 ml, 0.21 mol) in acetone (200 ml). The reaction mixture was stirred under an atmosphere of hydrogen gas at 414 kPa (60 psi). After stirring for 16 hours the reaction mixture was filtered through Arbocel (trade mark) and the solvent removed under reduced pressure to give the title compound (15 ml) as a thin oil.