Reacción #1016773

ord-be31e564d1204591b92eacae595bedb5

Ecuación de reacción

CC(C)(C)NCc1cc(-c2ccc(Cl)c(Cl)c2)cc(-c2ccc(Cl)c(Cl)c2)c1O.Cl
Intermediate 5
CC(C)(C)NCc1cc(-c2ccc(Cl)c(Cl)c2)cc(-c2ccc(Cl)c(Cl)c2)c1O.Cl
5′-((tert-Butylamino)methyl)-3,3″,4,4″-tetrachloro-[1,1′:3′,1″-terphenyl]-4′-ol hydrochloride
O=Cc1cc(Br)cc(Br)c1O
3,5-dibromosalicylaldehyde
O=Cc1cc(-c2ccc(Cl)c(Cl)c2)cc(-c2ccc(Cl)c(Cl)c2)c1O
3,3″,4,4″-Tetrachloro-4′-hydroxy-[1,1′:3′,1″-terphenyl]-5′-carbaldehyde

Condiciones de reacción

Condiciones detalladas
See reaction.notes.procedure_details.

Procedimiento

3,3″,4,4″-Tetrachloro-4′-hydroxy-[1,1′:3′,1″-terphenyl]-5′-carbaldehyde was prepared using the procedure described in Intermediate 5 from 3,5-dibromosalicylaldehyde and 3,4-chlorophenylboronic acid.

Fuente

DOI: 10.6084/m9.figshare.5104873.v1Patente: US09296696B2uspto-grants-2016_03