Reaction #992684

Reaction equation

3-Amino-1,2,4-triazole

Trifluoroacetic acid

→

3-Amino-1,2,4-Triazolium TFA

Solvents

water

Conditions

Workup

1. 1
   OtherThe water was removed in vacuo
2. 2
   Temperaturewith heating to approximately 90° C. for 4 hours

Procedure

3-Amino-1,2,4-triazole (1.27 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

Source