Reaction #94885

Reaction equation

2-diethylaminoethyl chloride hydrochloride

1-[2-Chloro-4-(2-diethylaminoethoxy)phenyl]-1-butanone

3-dimethylamino-2-methylpropyl chloride hydrochloride

→

1-[2-Chloro-4-(3-dimethylamino-2-methylpropoxy)phenyl]-1-butanone

Conditions

Workup

1. 1
   OtherThis compound is prepared by essentially the same procedure
2. 2
   OtherThe product is obtained as a colorless oil upon distillation in vacuo (0.3 mm.)

Procedure

This compound is prepared by essentially the same procedure as described in Example 1 Step A except that the 2-diethylaminoethyl chloride hydrochloride of Example 1 Step A is replaced by an equimolecular quantity of 3-dimethylamino-2-methylpropyl chloride hydrochloride. The product is obtained as a colorless oil upon distillation in vacuo (0.3 mm.).

Source