Reaction #944006
ord-2aebb45d1c4140a6b49f0659aa90cf3d
Reaction equation
α-(4-difluoromethoxyphenyl)-α-(4-methylsulfonylanilino)acetonitrile
crotonaldehyde
→
title compound
α-(4-Difluoromethoxyphenyl)-α-(4-methylthioanilino)acetonitrile
Reagents
None
Conditions
Detailed conditions
See reaction.notes.procedure_details.
Procedure
Following a procedure similar to that described in Example 1(iii), but using α-(4-difluoromethoxyphenyl)-α-(4-methylsulfonylanilino)acetonitrile [prepared as described in step (ii) above] and crotonaldehyde as starting materials, the title compound was obtained as a white powder (yield 31%), melting at 98-99° C.