Reaction #943995

ord-fcbdbaec14734beb8ea06418f985b35f

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Following a procedure similar to that described in Example 1(iii), but using α-(4-methylphenyl)-α-(4-sulfamoylanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as a brown powder (yield 13%), melting at 183-184° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE039420E1uspto-grants-2006_12