Reaction #927267

ord-3e917755f873453e9da0451521c08301

Solvents

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

A solution of 2-octylcycloprop-2-ene-1-carboxylic acid (350 mg, 1.8 mmol) in ether was treated with 0.45 g (3.5 mmol) of oxalyl chloride at room temperature. The reaction mixture was stirred for one hour then stripped to give 330 mg of 2-octylcycloprop-2-ene-1-carbonyl chloride.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06365549B2uspto-grants-2002_04