Reaction #926548

ord-2c682cd16e3a4ca5adf89dfa3adcaa91

Reaction equation

Nc1c(I)cc(I)c(C(=O)O)c1I
2,4,6-triiodo-3-amino-benzoic acid
O=C(Cl)CCN1C(=O)c2ccccc2C1=O
β-phthalimidopropionic acid chloride
→
NCCC(=O)Nc1c(I)cc(I)c(C(=O)O)c1I
2,4,6-triiodo-3-β-aminopropionylamino-benzoic acid

Reactants

Nc1c(I)cc(I)c(C(=O)O)c1I
2,4,6-triiodo-3-amino-benzoic acid
O=C(Cl)CCN1C(=O)c2ccccc2C1=O
β-phthalimidopropionic acid chloride

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The same procedure is used as for Compond I, using 2,4,6-triiodo-3-amino-benzoic acid as iodo starting material and β-phthalimidopropionic acid chloride.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04094966uspto-grants-1978_06