Reaction #86630

ord-edb312ea6ca14b7db0bf8d5eba753988

Reaction equation

C=CCCCCCCCCCOC(=O)C(C)(C)Br
10-undecenyl 2-bromo-2-methylpropanate
CCO[Si](CCCS)(OCC)OCC
3-mercaptopropyltriethoxysilane
→
CCO[Si](CCCSCCCCCCCCCCCOC(=O)C(C)(C)Br)(OCC)OCC
11-(3-(triethoxysilyl)propylthio)undecyl 2-bromo-2-methylpropanate

Reactants

C=CCCCCCCCCCOC(=O)C(C)(C)Br
10-undecenyl 2-bromo-2-methylpropanate
CCO[Si](CCCS)(OCC)OCC
3-mercaptopropyltriethoxysilane

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The 10-undecenyl 2-bromo-2-methylpropanate was reacted with 3-mercaptopropyltriethoxysilane in the same manner as in Example 1 to give 11-(3-(triethoxysilyl)propylthio)undecyl 2-bromo-2-methylpropanate of the chemical formula below (compound 5).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09434794B2uspto-grants-2016_09