Reaction #821334

ord-02cd26076f4944fcb1da7dcd39b0dc3f

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The 2-(4-nitro-3-methylphenylamino)propane-1,3-diol (11) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07591860B2uspto-grants-2009_09