Reaction #821332

ord-3ab4aab80cdb48e1b4f6f93578b840de

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The 3-(4-nitro-3-methylphenylamino)propane-1,2-diol (9) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07591860B2uspto-grants-2009_09