Reaction #817429

Reaction equation

4-trifluoromethyl-benzene-1,2-diamine

benzo[b]thiophene-2-sulfonyl chloride

→

N,N′-(4-Trifluoromethyl-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide)

Yield 53.3%

Conditions

Procedure

N,N′-(4-Trifluoromethyl-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide) (100 mg) was prepared by using 4-trifluoromethyl-benzene-1,2-diamine (0.06 g, 0.33 mmol) and benzo[b]thiophene-2-sulfonyl chloride (0.157 g, 0.67 mmol), following procedure as in Example 32.

Source