Reaction #817428

Reaction equation

4,5-dichloro-benzene-1,2-diamine

Benzo[b]thiophene-2-sulfonyl chloride

→

N,N′-(4,5-Dichloro-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide)

Yield 63.8%

Conditions

Procedure

N,N′-(4,5-Dichloro-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide) (120 mg) was prepared by using 4,5-dichloro-benzene-1,2-diamine (0.06 g, 0.33 mmol) and Benzo[b]thiophene-2-sulfonyl chloride (0.157 g, 0.67 mmol), following procedure as in Example 32.

Source