Reaction #817425

ord-db0ae80c01974b2380efa80cc9cc72c1

Reaction equation

Nc1ccc(Br)cc1N
4-bromobenzene-1,2-diamine
O=S(=O)(Cl)c1cc2ccccc2s1
benzothiophene-2-sulfonyl chloride
O=S(=O)(Nc1ccc(Br)cc1NS(=O)(=O)c1cc2ccccc2s1)c1cc2ccccc2s1
N,N′-(4-bromo-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide)

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

N,N′-(4-bromo-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide) (255 mg) was prepared as in Example 31 using 4-bromobenzene-1,2-diamine and benzothiophene-2-sulfonyl chloride as requisite starting materials.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07582673B2uspto-grants-2009_09