Reaction #817424

ord-203249a7db0e46da906554fd852d7d7c

Reaction equation

Nc1ccc(Cl)cc1N
4-chlorobenzene-1,2-diamine
O=S(=O)(Cl)c1cc2ccccc2s1
benzothiophene-2-sulfonyl chloride
→
O=S(=O)(Nc1ccc(Cl)cc1NS(=O)(=O)c1cc2ccccc2s1)c1cc2ccccc2s1
N,N′-(4-chloro-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide)

Reactants

Nc1ccc(Cl)cc1N
4-chlorobenzene-1,2-diamine
O=S(=O)(Cl)c1cc2ccccc2s1
benzothiophene-2-sulfonyl chloride

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

N,N′-(4-chloro-1,2-phenylene)bis(1-benzothiophene-2-sulfonamide) (310 mg) was prepared as in Example 31 using 4-chlorobenzene-1,2-diamine and benzothiophene-2-sulfonyl chloride as requisite starting materials.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07582673B2uspto-grants-2009_09