Reaction #78126

ord-18fb540115da47d59cd7445896f2951e

Reaction equation

Nc1cnccc1NCC1CCN(c2ccncc2)CC1
N4-[1-(4-pyridyl)piperidin-4-ylmethyl]-3,4-pyridinediamine
COc1ccc(C(=O)Cl)cc1
4-methoxybenzoyl chloride
COc1ccc(C(=O)Nc2cnccc2NCC2CCN(c3ccncc3)CC2)cc1
title compound
Yield 6.2%
COc1ccc(C(=O)Nc2cnccc2NCC2CCN(c3ccncc3)CC2)cc1
N3-(4-methoxybenzoyl)-N4-[1-(4-pyridyl)piperidin-4-ylmethyl]-3,4-pyridinediamine
Yield 6.2%

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using a similar procedure to that described in Example 2, Part D, N4-[1-(4-pyridyl)piperidin-4-ylmethyl]-3,4-pyridinediamine (110 mg, 0.388 mmol) and 4-methoxybenzoyl chloride (0.66 mL, 0.388 mmol) yielded 10 mg (6%) of the title compound as a hydrochloride salt.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06710057B2uspto-grants-2004_03