Reaction #75290

ord-c507f2867afc4396a8193fc0532cd35c

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe slightly exothermic reaction
  2. 2
    Otherwas accompanied by the precipitation of the solid N-phenacylpyridinium bromide
  3. 3
    FiltrationThe salt was then filtered
  4. 4
    Washwashed thoroughly with anhydrous ether

Procedure

N-phenacylpyridinium bromide was prepared by slowly adding phenacyl bromide to a stirred flask containing an equimolar quantity of pyridine. The slightly exothermic reaction was accompanied by the precipitation of the solid N-phenacylpyridinium bromide. The salt was then filtered and washed thoroughly with anhydrous ether.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04175963uspto-grants-1979_11