Reaction #75239

ord-87d8d09ce5804668a7dad94490cd33e9

Reaction equation

CCCCCC(O)CCCCl
1-chloro-4-nonanol
CC(=O)OC(C)=O
acetic anhydride
→
CCCCCC(CCCCl)OC(C)=O
1-Chloro-4-acetoxynonane

Reactants

CCCCCC(O)CCCCl
1-chloro-4-nonanol
CC(=O)OC(C)=O
acetic anhydride

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Temperatureis heated on a steam bath for 11/2 hours

Procedure

A mixture of 1-chloro-4-nonanol (111.99 g.; 0.627 mole) and acetic anhydride (128.0 g.; 1.254 moles) is heated on a steam bath for 11/2 hours.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04175203uspto-grants-1979_11