Reaction #742257

ord-834acd19ff5041ad904f8c6a0c94fe5a

Reaction equation

CCN(CC)c1ccc(C(C)=CC(=O)OCCC(C)CCc2ccccc2)c(O)c1
3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid 3-methyl-5-phenyl-pentyl ester
CCOC(=O)C=C(C)c1ccc(N(CC)CC)cc1O
3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid ethyl ester
CC(CCO)CCc1ccccc1
3-methyl-5-phenyl-pentanol
→
CCN(CC)c1ccc(/C(C)=C/C(=O)OCCC(C)CCc2ccccc2)c(O)c1
(E)-3-(4-Diethylamino-2-hydroxy-phenyl)-but-2-enoic acid 3-methyl-5-phenyl-pentyl ester

Reactants

CCN(CC)c1ccc(C(C)=CC(=O)OCCC(C)CCc2ccccc2)c(O)c1
3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid 3-methyl-5-phenyl-pentyl ester
—
tetraisopropyl-o-titanate
CCOC(=O)C=C(C)c1ccc(N(CC)CC)cc1O
3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid ethyl ester
CC(CCO)CCc1ccccc1
3-methyl-5-phenyl-pentanol

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

According to the same procedure, 3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid 3-methyl-5-phenyl-pentyl ester was prepared from 3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid ethyl ester, 3-methyl-5-phenyl-pentanol and tetraisopropyl-o-titanate.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE043006E1uspto-grants-2011_12