Reaction #72622

ord-32e71a3988a4437a87cb45c5c4dac5fa

Reaction equation

N#CC1=C(N)CCCC1
2-aminocyclohex-1-enecarbonitrile
O=C(N=C=S)c1ccccc1
benzoyl isothiocyanate
→
N#CC1=C(NC(=S)NC(=O)c2ccccc2)CCCC1
N-(2-Cyanocyclohex-1-enylcarbamothioyl)benzamide

Reactants

N#CC1=C(N)CCCC1
2-aminocyclohex-1-enecarbonitrile
O=C(N=C=S)c1ccccc1
benzoyl isothiocyanate

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Prepared as in Example 1a from 2-aminocyclohex-1-enecarbonitrile (Example 10b) and benzoyl isothiocyanate as a white solid. MS 286 (MH+).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08541421B2uspto-grants-2013_09