Reaction #71591

ord-9801c11d98dc42678e03398f0533c4eb

Reaction equation

CC1=C(/C=C/C(C)=C/C=C/C(C)=C/C(=O)O)C(C)(C)CCC1
retinoic acid
→
CC1=C(/C=C/C(C)=C\C=C\C(C)=C\C(=O)O)C(C)(C)CCC1
9-(Z)-retinoic Acid

Reactants

CC1=C(/C=C/C(C)=C/C=C/C(C)=C/C(=O)O)C(C)(C)CCC1
retinoic acid

Reagents

None

Solvents

CC(C)O
isopropanol

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Temperaturerefluxed

Procedure

The raw retinoic acid thus obtained was suspended in 235.5 g (300 ml) isopropanol (w=1.0) and refluxed.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08536373B2uspto-grants-2013_09