Reaction #696702

ord-48795fde0e514c28afb9751c2a4e4355

Reaction equation

CC(C)(C#N)N=NC(C)(C)C#N
azobisisobutyronitrile
C=C(C)C(=O)OCCCCCCCCCCCC
lauryl methacrylate
C=CN1CCCC1=O
N-vinyl-2-pyrrolidone
→
C=C(C)C(=O)OCCCCCCCCCCCC.C=CN1CCCC1=O
N-vinyl-2-pyrrolidone lauryl methacrylate

Reactants

CC(C)(C#N)N=NC(C)(C)C#N
azobisisobutyronitrile
—
Solvent L
C=C(C)C(=O)OCCCCCCCCCCCC
lauryl methacrylate
C=CN1CCCC1=O
N-vinyl-2-pyrrolidone

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe mixture was reacted at 60 to 70° C. for about 12 hours at nitrogen atmosphere

Procedure

The N-vinyl-2-pyrrolidone/lauryl methacrylate (6/94) copolymer was prepared in the following manner. In 100 parts of 0-grade Solvent L were placed 47 parts of lauryl methacrylate, 3 parts of N-vinyl-2-pyrrolidone and 0.2 parts of azobisisobutyronitrile (polymerization initiator). The mixture was reacted at 60 to 70° C. for about 12 hours at nitrogen atmosphere.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05998075uspto-grants-1999_12