Reaction #684940

Reaction equation

sodium hydroxide

4-hydroxy-4′-(di-p-tolylamino)stilbene

glycidyl methacrylate

→

1,2-dihydroxy-3-[4′-(di-p-tolylamino)stilbene-4-yloxy]propane

Solvents

toluene

triethylamine

toluene

Conditions

Workup

1. 1
   OtherIn a reaction vessel equipped with a stirrer
2. 2
   workup.STIRRINGthe mixture is further agitated for 8 hours at 95° C.

Procedure

In a reaction vessel equipped with a stirrer, a thermometer, a condenser, and a dropping funnel, 11.75 g of 4-hydroxy-4′-(di-p-tolylamino)stilbene, 4.35 g of glycidyl methacrylate, and 8 ml of toluene are contained, and the mixture is heated to 90° C. Further, 0.16 g of triethylamine is added thereto, and the mixture is agitated for 8 hours at 95° C. Next, 16 ml of toluene and 20 ml of a 10% aqueous solution of sodium hydroxide are added thereto, and the mixture is further agitated for 8 hours at 95° C.

Source