Reaction #67832

ord-ce33ff6cdcf4458b8e73e898d1d7b990

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherLC/MS [6.90 min; 450 (M+1)]

Procedure

3-[(2-fluoro-4-iodophenyl)amino]-N′-pyridin-2-ylisonicotinohydrazide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.5 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 0.8 mmol of pyridin-2-yl-hydrazine. LC/MS [6.90 min; 450 (M+1)]

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08524911B2uspto-grants-2013_09