Reaction #65830

ord-7847c01625e040a0b1c90b096b774219

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using an analogous procedure to that described in Example 3 except that diisopropylethylamine was used in place of potassium carbonate, 3-methoxy-3-[3-(1-methyl-2-oxo-1,2-dihydroquinolin-6-ylmethoxy)phenyl]pyrrolidine was reacted with 2-propynyl bromide to give 3-methoxy-3-[3-(1-methyl-2-oxo-1,2-dihydroquinolin-6-ylmethoxy)phenyl]-1-(prop-2-ynyl)pyrrolidine as a gum in 21% yield.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05420298uspto-grants-1995_05