Reaction #596474

Reaction equation

4-(Benzylamino)-1-methylcyclohexanol

→

white solid

Yield 83.0%

4-amino-1-methylcyclohexanol

Yield 83.0%

Solvents

EtOH

Conditions

Workup

1. 1
   OtherThe resulting reaction liquid
2. 2
   Filtrationwas filtered
3. 3
   Concentrationconcentrated under reduced pressure
4. 4
   Otherdried under vacuum

Procedure

4-(Benzylamino)-1-methylcyclohexanol (335 mg, 1.53 mmol) was dissolved in EtOH (7.95 ml), followed by addition of Pd (10 wt % on activated carbon, 35 mg), and then the resulting liquid was stirred at room temperature under hydrogen stream for 31 hours. The resulting reaction liquid was filtered, concentrated under reduced pressure, and dried under vacuum, to obtain 164 mg of white solid (83%).

Source