Reaction #58083

ord-98c56282b497474784d067ae10f5098d

Reaction equation

COC(=O)c1cccc(C(=O)NN)c1
methyl 3-hydrazinocarbonyl-benzoate
CCOC(C)=N.Cl
ethyl acetimidate hydrochloride
→
COC(=O)c1cccc(C(=O)NNC(C)=N)c1
methyl 3-[N′-(1-imino-ethyl)-hydrazinocarbonyl]-benzoate

Reactants

—
product 1a
COC(=O)c1cccc(C(=O)NN)c1
methyl 3-hydrazinocarbonyl-benzoate
CCOC(C)=N.Cl
ethyl acetimidate hydrochloride

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherPrepared analogously to the method

Procedure

Prepared analogously to the method described for intermediate product 1a) from methyl 3-hydrazinocarbonyl-benzoate and ethyl acetimidate hydrochloride. White solid.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423036B2uspto-grants-2008_09