Reaction #56603
ord-b90eeb78e34d464d942b2a5c26b6dbe7
Reaction equation
Methyl 3-(5-chlorobenzotriazol-2-yl)-5-tert-butyl-4-hydroxyhydrocinnamate
1,2,2,6,6-pentamethyl-4-hydroxypiperidine
→
title compound
1,2,2,6,6-Pentamethylpiperidin-4-yl 3-(5-Chlorobenzotriazol-2-yl)-5-tert-butyl-4-hydroxyhydrocinnamate
Reactants
Reagents
None
Conditions
Detailed conditions
See reaction.notes.procedure_details.
Procedure
Methyl 3-(5-chlorobenzotriazol-2-yl)-5-tert-butyl-4-hydroxyhydrocinnamate (10.0 g, 0.026 mol) and 1,2,2,6,6-pentamethyl-4-hydroxypiperidine (3.98 g, 0.023 mol) are reacted together according to the procedure of Example 1. The title compound is obtained in a yield of 3.23 g (26%) as an off-white solid, melting at 150-158° C., whose structure is consistent with 1Hnmr and mass spectrometry. The compound has a molar absorptivity of 17,092 l/mole cm.