Reaction #549345

ord-af2f4aab4300402fa9ec1f56a11db220

Reaction equation

Nc1c(I)cc(I)c(C(=O)O)c1I
2,4,6-triiodo-3-amino-benzoic acid
O=C(Cl)CCN1C(=O)c2ccccc2C1=O
β-phthalimidopropionic acid chloride
→
NCCC(=O)Nc1c(I)cc(I)c(C(=O)O)c1I
2,4,6-triiodo-3-β-aminopropionylaminobenzoic acid

Reactants

—
Compound I
Nc1c(I)cc(I)c(C(=O)O)c1I
2,4,6-triiodo-3-amino-benzoic acid
O=C(Cl)CCN1C(=O)c2ccccc2C1=O
β-phthalimidopropionic acid chloride

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The same procedure is used as for Compound I, using 2,4,6-triiodo-3-amino-benzoic acid as iodo starting material and β-phthalimidopropionic acid chloride.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04065553uspto-grants-1977_12