Reaction #548060

ord-87efd3f8a46b4bc18c3fff6d5d0b8772

Reaction equation

NS(=O)(=O)OCCOS(N)(=O)=O
1,2-bis-O-sulfamyl-1,2-ethanediol
OCCCCCCCCCCO
1,10-decanediol
→
NS(=O)(=O)OCCCCCCCCCCOS(N)(=O)=O
1,10-Bis-O-sulfamyl-1,10-decanediol

Reactants

NS(=O)(=O)OCCOS(N)(=O)=O
1,2-bis-O-sulfamyl-1,2-ethanediol
OCCCCCCCCCCO
1,10-decanediol
—
alkanediol

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

1,10-Bis-O-sulfamyl-1,10-decanediol is prepared in the same manner as 1,2-bis-O-sulfamyl-1,2-ethanediol in Example 1 except that 1,10-decanediol (67 g., 0.385 mol.) is employed as the alkanediol.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04061663uspto-grants-1977_12