Reaction #51764

Reaction equation

5-Isopropyl-2-nitro-4-thiocyanato-phenylamine

hydrogen

→

4-Isopropyl-5-thiocyanato-benzene-1,2-diamine

Solvents

THF

Conditions

Procedure

5-Isopropyl-2-nitro-4-thiocyanato-phenylamine (prepared in Example QQ-1; 7.83 g, 33 mmol) was hydrogenated using Raney nickel (2 g) and THF (100 mL) in the presence of hydrogen (50 psi) as described in General Method 3. MS(APCI): 208(M+H).

Source