Reaction #516688

ord-3b366d82d196420a9bd95ad4ab7820fd

Reaction equation

Cc1cc(O)cc(O)c1
Orcinol
CCCCCCNCCCCCC
di-n-hexylamine
→
CCCCCCN(CCCCCC)c1cc(C)cc(O)c1
1-di-n-hexylamino-3-methyl-5-hydroxybenzene

Reactants

Cc1cc(O)cc(O)c1
Orcinol
CCCCCCNCCCCCC
di-n-hexylamine

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Orcinol (5-resorcinol) was aminized by di-n-hexylamine, so as to obtain 1-di-n-hexylamino-3-methyl-5-hydroxybenzene. The hydroxy group thereof was etherized with methyl iodide, and then nitrosoized so as to obtain 1-di-n-hexylamino-3-methyl-4-nitroso-5-methoxybenzene.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06316605B1uspto-grants-2001_11