Reaction #511640

ord-535ac1a8fe8f44c28e3893af634bb01b

Reaction equation

Oc1ccc(Cc2nc3c(Cc4ccccc4)nc(-c4ccc(O)cc4)cn3c2O)cc1
coelenterazine
O=C(O)CN(CCN(CC(=O)O)CC(=O)O)CC(=O)O
EDTA
O=S(=O)(O)CCN1CCN(CCO)CC1
Hepes
[Cl-].[K+]
KCl
CCC(CC)COC(C(=O)N(C)CC[NH+](C)C)(c1ccccc1)c1ccccc1.[Cl-]
X-100
Oc1ccc(Cc2nc3c(Cc4ccccc4)nc(-c4ccc(O)cc4)cn3c2O)cc1
coelenterazine
Oc1ccc(Cc2nc3c(Cc4ccccc4)nc(-c4ccc(O)cc4)cn3c2O)cc1
coelenterazine
Oc1ccc(Cc2nc3c(Cc4ccccc4)nc(-c4ccc(O)cc4)cn3c2O)cc1
coelenterazine
COc1c(Cc2ccccc2)nc2c(Cc3ccccc3)nc(-c3ccccc3)cn12
2,8-Dibenzyl-3-methoxy-6-phenyl-imidazo[1,2-a]pyrazine

Solvents

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Chemiluminescence of P450 altered coelenterazine or coelenterazine derivatives was determined immediately following addition of 80 microliter of 37.5 mM Hepes pH7.4; 625 mM KCl; 0.125 mM EDTA pH 8.0; 0.25% Triton X-100; 0.125% Mazu; 1.25% Glycerol; 0.25 mg/mL gelatin to the P450 reactions. Renilla luciferase (1.2 ng/mL) (purchased from Chemicon) was added for detection of bioluminescence of P450 altered coelenterazine or coelenterazine derivatives.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08106052B2uspto-grants-2012_01