Reaction #487528

ord-768740c8253947a09478f0ca8eb919de

Reaction equation

CCCCCCCC/C=C\CCCCCCCCO
Oleyl alcohol
C=CCCCCCCCC(=O)O
9-decenoic acid
→
C=CCCCCCCCC(=O)OCCCCCCCCC=CCCCCCCCC
Compound E
Yield 96.0%
C=CCCCCCCCC(=O)OCCCCCCCCC=CCCCCCCCC
Octadec-9-enyl dec-9-enoate
Yield 96.0%

Reactants

CCCCCCCC/C=C\CCCCCCCCO
Oleyl alcohol
C=CCCCCCCCC(=O)O
9-decenoic acid
—
compound E

Reagents

None

Solvents

CCCCCC.CCOC(C)=O
Ethyl acetate Hexane

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Compound E was prepared from Oleyl alcohol and 9-decenoic acid following the general procedure previously discussed and shown in FIG. 10. Pure compound E was a colorless oil obtained by column chromatography with Ethyl acetate/Hexane=1:40.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08741822B2uspto-grants-2014_06