Reaction #480319

ord-811b43e5184f404e916b495f1de84d2c

Reaction equation

COC(=O)C(=O)c1ccccc1
methyl phenylglyoxalate
CCCCCCO
1-hexanol
CCCCCCOC(=O)C(=O)c1ccccc1
hexyl phenylglyoxalate
Yield 87.0%

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

16.42 g (0.1 mol) of methyl phenylglyoxalate is transesterified as described in example 1.1, using 1-hexanol instead of methoxyethanol. 21.33 g (87%) hexyl phenylglyoxalate are obtained as a colorless liquid.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06806024B1uspto-grants-2004_10