Reaction #4718

ord-e4dccccf09ef4bc5a00c348cf634def8

Reaction equation

NNC(=O)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-hydrazine carboxamide
O=C=NCc1ccccc1
benzyl isocyanate
→
O=C(NCCCOc1cccc(CN2CCCCC2)c1)NNC(=O)NCc1ccccc1
N-Benzyl-N'-[3-[3-(1-piperidinylmethyl)-phenoxy]propyl]1,2-hydrazine dicarboxamide

Reactants

NNC(=O)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-hydrazine carboxamide
O=C=NCc1ccccc1
benzyl isocyanate

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The compound is prepared by a method analogous to that of Example 20 from N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-hydrazine carboxamide and benzyl isocyanate. The analytical values are summarized in Table I.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04727081uspto-grants-1988_02