Reaction #4707

ord-c8badcb2ff2d4488bfd347f19c735655

Reaction equation

NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-hydrazine carbothioamide
CC(C)N=C=O
isopropyl isocyanate
→
CC(C)NC(=O)NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-Isopropyl-2-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]aminothioxomethyl]hydrazine carboxamide

Reactants

NNC(=S)NCCCOc1cccc(CN2CCCCC2)c1
N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-hydrazine carbothioamide
CC(C)N=C=O
isopropyl isocyanate

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The compound is prepared by a method analogous to that of Example 9 from N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-hydrazine carbothioamide and isopropyl isocyanate. The analytical values are summarized in Table I.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04727081uspto-grants-1988_02