Reaction #459687

Reaction equation

1-chloro-9,9,9-trifluoro-4-nonanol

1-chloro-4-acetoxynonane

amyl bromide

1-chloro-9,9,9-trifluoro-4-nonanone

→

1-Chloro-4-acetoxy-9,9,9-trifluorononane

Conditions

Workup

1. 1
   Otherthere is obtained in succession

Procedure

By following the procedure described for 1-chloro-4-acetoxynonane (Example A) but substituting 1-bromo-5,5,5-trifluoropentane for amyl bromide, there is obtained in succession: 1-chloro-9,9,9-trifluoro-4-nonanone, 1-chloro-9,9,9-trifluoro-4-nonanol, and 1-chloro-4-acetoxy-9,9,9-trifluoronane.

Source