Reaction #44319

ord-0f6b71fde1054d1daa9c9fbeee5c6366

Solvents

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    workup.DISSOLUTIONwere completely dissolved
  2. 2
    workup.STIRRINGthe result was stirred for 3 hours
  3. 3
    OtherWhite powder on the surface of the result was collected
  4. 4
    Washwashed three times each with distilled water

Procedure

7.5 g of stearic acid and 1.2 g of sodium hydroxide were added to 300 ml of water and sufficiently stirred until they were completely dissolved. 5.2 g of silver nitrate was added thereto, and the result was stirred for 3 hours. White powder on the surface of the result was collected and washed three times each with distilled water and with methanol to obtain silver stearate. An anode active material was prepared as in Example 1, except that silver stearate was used instead of nickel stearate, the molar ratio of silver to silicon was 0.2:1, the weight ratio of silicon to graphite was 0.5:1, and the carbon layer was 5.2 wt % of the anode active material.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07736804B2uspto-grants-2010_06